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Beilstein J. Org. Chem. 2013, 9, 1443–1447, doi:10.3762/bjoc.9.163
Graphical Abstract
Scheme 1: SmI2-mediated cyclisations directed by a C–Si bond.
Scheme 2: Reduction of a spirocyclic lactone using SmI2−H2O−Et3N.
Scheme 3: Stereoselective spirocyclisation of functionalised keto-lactone substrates directed by a C–Si bond.
Scheme 4: Telescoped stereoselective spirocyclisation/lactone reduction.
Scheme 5: Telescoped stereoselective spirocyclisation/lactone reduction/Peterson elimination.